ËÜ»¯¼Á£¬£¬£¬£¬£¬£¬£¬£¬¼´ÁÚ±½¶þ¼×Ëáõ¥ÀàÔöËܼÁ£¬£¬£¬£¬£¬£¬£¬£¬¼ò³ÆPAEs¡£¡£¡£¡£¡£¡£Ëü±»ÆÕ±éÓ¦ÓÃÓÚÍæ¾ß¡¢Ê³Îï°ü×°¡¢ÒÒÏ©µØ°å¡¢±ÚÖ½¡¢Çå½à¼Á¡¢Ö¸¼×ÓÍ¡¢ÅçÎí¼Á¡¢Ï´·¢Ë®ºÍãåÔ¡ÒºµÈÊý°ÙÖÖ²úÆ·ÖС£¡£¡£¡£¡£¡£
ʳÎïÖеÄËÜ»¯¼ÁȪԴÖ÷ÒªÓÐÈý¸ö·½Ã棺һÊÇͨ¹ýÇéÐÎǨáãÖÁʳÎïÁ´£¬£¬£¬£¬£¬£¬£¬£¬¶þÊÇͨ¹ýʳÎïËÜÁϰüװǨáãÖÁʳÎ£¬£¬£¬£¬£¬£¬£¬ÈýÊDz»·¨Ìí¼ÓÖÁʳÎïÖС£¡£¡£¡£¡£¡£ËÜ»¯¼ÁÊôÇéÐκɶûÃÉ£¬£¬£¬£¬£¬£¬£¬£¬ÒѳÉΪȫÇòÐÔµÄÖ÷ÒªÇéÐÎÓлúÎÛȾÎ£¬£¬£¬£¬£¬£¬£¬ºã¾ÃÉãʳËÜ»¯¼Á¶ÔÄÐÐÔÉúÖ³Á¦µÄÓ°Ïì½Ï´ó£¬£¬£¬£¬£¬£¬£¬£¬¿ÉÄÜÔì³ÉСº¢ÐÔ±ðÅÓÔÓ¡£¡£¡£¡£¡£¡£ÔÚÌåÄÚºã¾ÃÐî»ý»áµ¼Ö»ûÐΡ¢°©±äºÍÍ»±ä¡£¡£¡£¡£¡£¡£±ðµÄ£¬£¬£¬£¬£¬£¬£¬£¬¶ÔÐÄѪ¹Ü¡¢Ïû»¯ºÍÃÚÄòϵͳҲÓкܴóΣÏÕ¡£¡£¡£¡£¡£¡£
luck18¹ÙÍøÒÇÆ÷²ÎÕÕ¹ú±êGB/T 21911-2008¡¶Ê³ÎïÖÐÁÚ±½¶þ¼×Ëáõ¥µÄ²â¶¨¡·£¬£¬£¬£¬£¬£¬£¬£¬Öƶ©ÁËʹÓÃÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒÇ£¨GC-MS 6800£©²â¶¨Ê³ÎïÖеÄËÜ»¯¼ÁµÄ¼ì²â¼Æ»®£¬£¬£¬£¬£¬£¬£¬£¬±¾²âÊԼƻ®ÊÊÓÃÓÚʳÓÃÓÍ¡¢ÒûÁÏ¡¢¾ÆÀàµÈʳÎïÖеÄËÜ»¯¼Á¼ì²â£¬£¬£¬£¬£¬£¬£¬£¬²âÊÔЧ¹ûÖª×ãʳÎïÐÐÒµËÜ»¯¼ÁÏÞÁ¿ÏµIJâÊÔÒªÇ󡣡£¡£¡£¡£¡£
1¡¢Ê³ÎïÖÐËÜ»¯¼Á²âÊÔÒªÁì
²ÎÕÕ¹ú¼Ò±ê×¼GB/T 21911-2008¡¶Ê³ÎïÖÐÁÚ±½¶þ¼×Ëáõ¥µÄ²â¶¨¡·£¬£¬£¬£¬£¬£¬£¬£¬ÖÖÖÖʳÎï¾ÌáÈ¡¡¢¾»»¯ºó£¬£¬£¬£¬£¬£¬£¬£¬ÓÃGC-MS 6800ÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒǾÙÐвⶨ£¬£¬£¬£¬£¬£¬£¬£¬½ÓÄÉÌØÕ÷Ñ¡ÔñÀë×Ó¼ì²âɨÃèģʽ£¬£¬£¬£¬£¬£¬£¬£¬ÒÔË鯬µÄƷò±È¶¨ÐÔ£¬£¬£¬£¬£¬£¬£¬£¬¶¨Á¿Àë×ÓÍâ±ê·¨¶¨Á¿¡£¡£¡£¡£¡£¡£
£¨1£©²»º¬ÓÍÖ¬ÊÔÑù
Á¿È¡»ìÏýÔȳÆÒºÌåÊÔÑù5.0ml£¨º¬ÓжþÑõ»¯Ì¼µÄÊÔÑùÐèÏȳýÈ¥¶þÑõ»¯Ì¼£©£¬£¬£¬£¬£¬£¬£¬£¬¼ÓÈëÕý¼ºÍé2.0ml£¬£¬£¬£¬£¬£¬£¬£¬Õñµ´1min£¬£¬£¬£¬£¬£¬£¬£¬¾²Ö÷ֲ㣨ÈôÓÐÐëҪʱÑÎÎö»òÓÚ4000r/minÀëÐÄ5min£©£¬£¬£¬£¬£¬£¬£¬£¬È¡ÉϲãÇåÒº¾ÙÐÐgcmsÆÊÎö¡£¡£¡£¡£¡£¡£
³ÆÈ¡»ìÏýÔȳƹÌÌå»ò°ë¹ÌÌåÊÔÑù5.00g£¬£¬£¬£¬£¬£¬£¬£¬¼ÓÊÊÁ¿Ë®£¨ÊÓÊÔÑùË®·Öº¬Á¿¼ÓË®£¬£¬£¬£¬£¬£¬£¬£¬×ÜË®Á¿Ô¼50ml£©£¬£¬£¬£¬£¬£¬£¬£¬Õñµ´30min£¬£¬£¬£¬£¬£¬£¬£¬Ò¡ÔÈ¡£¡£¡£¡£¡£¡£¾²ÖùýÂË£¬£¬£¬£¬£¬£¬£¬£¬È¡ÂËÒº25.0ml£¬£¬£¬£¬£¬£¬£¬£¬¼ÓÈëÕý¼ºÍé5.0ml£¬£¬£¬£¬£¬£¬£¬£¬Õñµ´1min£¬£¬£¬£¬£¬£¬£¬£¬¾²Ö÷ֲ㣨ÈôÓÐÐëҪʱÑÎÎö»òÓÚ4000r/minÀëÐÄ5min£©£¬£¬£¬£¬£¬£¬£¬£¬È¡ÉϲãÇåÒº¾ÙÐÐgcmsÆÊÎö¡£¡£¡£¡£¡£¡£
£¨2£©º¬ÓÍÖ¬ÊÔÑù
³ÆÈ¡»ìÏýÔȳƴ¿ÓÍÖ¬ÊÔÑù0.50g£¨×¼È·ÖÁ0.1mg£©£¬£¬£¬£¬£¬£¬£¬£¬ÓÃÒÒËáÒÒõ¥£º»·¼ºÍ飨Ìå»ý±È1:1£©¶¨ÈÝÖÁ10.0ml£¬£¬£¬£¬£¬£¬£¬£¬ÎÐÐý»ìÏý2min£¬£¬£¬£¬£¬£¬£¬£¬0.45umÂËĤ¹ýÂË£¬£¬£¬£¬£¬£¬£¬£¬ÂËÒº¾Äý½ºÉøÍ¸É«Æ××°Öþ»»¯£¬£¬£¬£¬£¬£¬£¬£¬ÍøÂçÁ÷³öÒº£¬£¬£¬£¬£¬£¬£¬£¬¼õѹŨËõÖÁ2.0ml£¬£¬£¬£¬£¬£¬£¬£¬¾ÙÐÐGCMSÆÊÎö¡£¡£¡£¡£¡£¡£
³ÆÈ¡»ìÏýÔȳƺ¬ÓÍÖ¬ÊÔÑù0.50g£¨×¼È·ÖÁ0.1mg£©ÓÚ¾ßÈûÈý½ÇÆ¿ÖУ¬£¬£¬£¬£¬£¬£¬£¬¼ÓÈë20mlʯÓÍÃÑÎÐÐý»ìÏý2min£¬£¬£¬£¬£¬£¬£¬£¬¾²ÖúóÌáȡʯÓÍÃѲ㣬£¬£¬£¬£¬£¬£¬£¬ÔÙÓÃʯÓÍÃÑÖØ¸´Ï´µÓÈý½ÇÆ¿ÖеIJÐÔüÈý´Î£¬£¬£¬£¬£¬£¬£¬£¬Ã¿´Î10ml£¬£¬£¬£¬£¬£¬£¬£¬ºÏ²¢ÌáȡҺ¾ÎÞË®ÁòËáÄÆ£¨10g£©¹ýÂË£¬£¬£¬£¬£¬£¬£¬£¬½«ÂËÒº¼õѹŨËõÖÁ¸É£¬£¬£¬£¬£¬£¬£¬£¬ÓÃÒÒËáÒÒõ¥£º»·¼ºÍ飨Ìå»ý±È1:1£©¶¨ÈÝÖÁ10.0ml£¬£¬£¬£¬£¬£¬£¬£¬ÎÐÐý»ìÏý2min£¬£¬£¬£¬£¬£¬£¬£¬0.45umÂËĤ¹ýÂË£¬£¬£¬£¬£¬£¬£¬£¬ÂËÒº¾Äý½ºÉøÍ¸É«Æ××°Öþ»»¯£¬£¬£¬£¬£¬£¬£¬£¬ÍøÂçÁ÷³öÒº£¬£¬£¬£¬£¬£¬£¬£¬Å¨ËõÖÁ2.0ml£¬£¬£¬£¬£¬£¬£¬£¬¾ÙÐÐGCMSÆÊÎö¡£¡£¡£¡£¡£¡£
2. ²âÊÔÒÇÆ÷
ÒÇÆ÷Ãû³Æ£ºÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒÇ
ÒÇÆ÷ÐͺţºGCMS6800
ÒÇÆ÷Ö÷ÒªÉèÖãºEIÀë×ÓÔ´¡£¡£¡£¡£¡£¡£
3. ²âÊÔÆ×ͼ
3.1 15ÖÖËÜ»¯¼Á»ìÏý±ê×¼ÈÜÒº×ÜÀë×ÓÁ÷¼à²âͼ£¨TIC£©ÈçÏÂËùʾ£º
1. ÁÚ±½¶þ¼×Ëá¶þ¼×õ¥£¨DMP£©£¬£¬£¬£¬£¬£¬£¬£¬2. ÁÚ±½¶þ¼×Ëá¶þÒÒõ¥ (DEP),3. ÁÚ±½¶þ¼×Ëá¶þÒì¶¡õ¥ (DIBP),4. ÁÚ±½¶þ¼×Ëá¶þ¶¡õ¥ (DBP),5. ÁÚ±½¶þ¼×Ëá¶þ£¨2-¼×Ñõ»ù£©õ¥ (DMEP),6. ÁÚ±½¶þ¼×Ëá¶þ£¨4-¼×Ñõ»ù-2-Îì»ù£©õ¥(BMPP),7. ÁÚ±½¶þ¼×Ëá¶þ£¨2-ÒÒÑõ»ù£©ÒÒõ¥ (DEEP),8. ÁÚ±½¶þ¼×Ëá¶þÎìõ¥ (DPP),9. ÁÚ±½¶þ¼×Ëá¶þ¼ºõ¥ (DHXP),10. ÁÚ±½¶þ¼×Ëá¶¡»ùÜлùõ¥ (BBP),11. ÁÚ±½¶þ¼×Ëᣨ2-¶¡Ñõ»ù£©ÒÒõ¥ (DBEP),12. ÁÚ±½¶þ¼×Ëá¶þ»·¼ºõ¥ (DCHP),13. ÁÚ±½¶þ¼×Ëá¶þ£¨2-ÒÒ»ù£©¼ºõ¥ £¨DEHP£©,14. ÁÚ±½¶þ¼×Ëá¶þÕýÐÁõ¥ (DNOP),15. ÁÚ±½¶þ¼×Ëá¶þÈÉõ¥ (DNP)¡£¡£¡£¡£¡£¡£
3.2ijÒûÁÏÑùÆ·ÖÐËÜ»¯¼Á²âÊÔ×ÜÀë×ÓÁ÷¼à²âͼ£¨TIC£©ÈçÏ£º
4.GCMS6800ÆøÏàÉ«Æ×ÖÊÆ×ÁªÓÃÒÇÏÈÈÝ
Ö÷ÒªÊÖÒÕ²ÎÊý£º
½øÑù¿Ú£º·ÖÁ÷/²»·ÖÁ÷
½øÑù¿Úζȣº×î¸ßʹÓÃζÈ450?C
µç×ÓѹÁ¦¿ØÖÆ£¨EPC£©¹æÄ££º0---50Psi, ¾«¶È0.1 Psi,Ö§³Öºãѹ,ºãÁ÷
×î´ó·ÖÁ÷±È£º500:1
ÖùÎÂÏä²Ù×÷ζȣºÊÒÎÂ+10?C---450?C
×î´óÉýÎÂËÙÂÊ£º40?C /min
ƽ̨ÉýΣº7½×8ƽ̨³ÌÐòÉýÎÂ
½øÑùÁ¿¹æÄ££º0.1---10uL
·åÃæ»ýÖØÏÖÐÔ£º< 1 % RSD
±£´æÊ±¼äÖØÏÖÐÔ£º< 0.5% RSD
´µÉ¨ÆøÁ÷Á¿£º2---10ml/min
×î´óÔËÐÐʱ¼ä£º999.99min
ÖÊÆ×ÊÖÒÕÖ¸±ê
Àë×Ó»¯ÄÜÁ¿(µç×Óºä»÷Ô´EI)£º 10 eV ---100eV£¨Í¨ÀýʹÓÃ70eV£¬£¬£¬£¬£¬£¬£¬£¬¿Éµ÷£©
ÖÊÁ¿¹æÄ££º1.5---1000amu
Çø·ÖÂÊ£º0.7 amu(°ë·å¿í)
Àë×ÓԴζȣº100---350¡æ
½Ó¿Ú×î¸ßʹÓÃζȣº 400¡æ
ÖÊÁ¿ÖáÎȹÌÐÔ£º +/-0.10 amu/48 hrs
ѸËÙ¶È£ºÈ«É¨Ã裬£¬£¬£¬£¬£¬£¬£¬1pg°Ë·úÝÁ£¨OFN£©ÔÚm/z 272´¦£¬£¬£¬£¬£¬£¬£¬£¬ÐÅÔë±È£¨S/N£©¡Ý30£º1 £¨RMS£©
ɨÃèËÙÂÊ£º×î¸ß10000amu/s
׼ȷ¶È£º 0.1 amu
Õæ¿Õϵͳ£º¸ßÐÔÄÜǰ¼¶»úе±Ã£¨¼¸ºÎ³éËÙΪ5m3/h£©ºÍÎÐÂÖ·Ö×ӱ㨼¸ºÎ³éËÙΪ67 l/s£©ÎªÖÊÆ×ϵͳÌṩÁË×ã¹»µÄÕæ¿ÕÌõ¼þ£¨¡Ü 8¡Á10-5 mbar£©£¬£¬£¬£¬£¬£¬£¬£¬¿í¹æÄ£µÄÕæ¿Õ¼ÆÌá¹©ÊµÊ±Õæ¿ÕÐÅÏ¢
¼ì²âÆ÷£º´ø¸ßÄÜ´òÄü«µÄµç×Ó±¶ÔöÆ÷
Èí¼þ¹¦Ð§£º
ÊÂÇéÕ¾Èí¼þ¿Éͬʱ¿ØÖÆÆøÏàÉ«Æ×ÒÇ¡¢×Ô¶¯½øÑùÆ÷ºÍÖÊÆ×ÒÇ£¬£¬£¬£¬£¬£¬£¬£¬Í¨¹ý¸ßËÙÍø¿¨ÊµÏÖÊý¾ÝÊÕÂÞÓë´«Ê䣻£»£»£»£»£»
¿ÉʵÏÖSIM¡¢ FULL SCAN¡¢MIXÈýÖÖɨÃèģʽ£»£»£»£»£»£»
Ö§³ÖÊÖ¶¯µ÷гºÍ×Ô¶¯µ÷г£»£»£»£»£»£»
ʵʱÏÔʾ×ÜÀë×ÓÁ÷Æ×ºÍÖÊÆ×ͼÆ×£»£»£»£»£»£»
¿É¿ìËÙÌáÈ¡Àë×ÓºÍȫɨÃèͼÆ×£»£»£»£»£»£»
Êý¾Ý´¦Öóͷ£Èí¼þ¿ÉÒÀ¾ÝÑùÆ·µÄÖÊÆ×ͼÔÚNIST2011Æ×¿âÖоÙÐÐÄ¿µÄ»¯ºÏÎï×Ô¶¯Õ÷²É,²¢ÏÔʾÕ÷²ÉЧ¹û.Õ÷²ÉЧ¹ûÏÔʾÿ¸ö»¯ºÏÎïµÄʵ²â±£´æÊ±¼ä¡¢·Ö×ӽṹʽÓë±ê׼ͼÆ×,È·ÈÏÀë×ÓÖ®¼äµÄ±ê׼Ʒò±ÈÓëʵ²âƷò±ÈµÈÒÔ¹©Ê¹ÓÃÕß׼ȷ¶¨ÐÔ¡¢¶¨Á¿ÆÊÎö¡£¡£¡£¡£¡£¡£